Carbaryl was analyzed in olive oil using solid phase extraction (SPE) with lanthanum silicate as a new solid sorbent followed by high performance liquid chromatography with UV-VIS detection (HPLC-UV). The various parameters influencing extraction such as different eluents, volumes of eluent, conditioning pH and several spiked concentrations were studied to determine the optimum conditions for lanthanum silicate- SPE. Mean recovery with methanol as eluent was 76% with RSD 2-3% in concentration range of 0.5-32 ppm. The limit of detection (LOD= 1.03 mg kg-1) was lower than maximum residue limit (MRL) established by WHO/FAO.
Maham, M., Kiarostami, V. (2017). Evaluation of Efficient Extraction Method for the Determination of Carbryl Residue in Olive Oil. Medbiotech Journal, 01(03), 118-121. doi: 10.22034/mbt.2017.86992
MLA
Mahdi Maham; Vahid Kiarostami. "Evaluation of Efficient Extraction Method for the Determination of Carbryl Residue in Olive Oil". Medbiotech Journal, 01, 03, 2017, 118-121. doi: 10.22034/mbt.2017.86992
HARVARD
Maham, M., Kiarostami, V. (2017). 'Evaluation of Efficient Extraction Method for the Determination of Carbryl Residue in Olive Oil', Medbiotech Journal, 01(03), pp. 118-121. doi: 10.22034/mbt.2017.86992
VANCOUVER
Maham, M., Kiarostami, V. Evaluation of Efficient Extraction Method for the Determination of Carbryl Residue in Olive Oil. Medbiotech Journal, 2017; 01(03): 118-121. doi: 10.22034/mbt.2017.86992